Journal of Guangxi Normal University(Natural Science Edition) ›› 2020, Vol. 38 ›› Issue (6): 82-87.doi: 10.16088/j.issn.1001-6600.2020.06.010

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Chemical Constituents of Ethyl Acetate Fraction of Blumea riparia (Bl.) DC.

CHEN Meian, JIANG Jianping*, MA Wenfang   

  1. College of Pharmacy, Guangxi University of Chinese Medicine, Nanning Guangxi 530001, China
  • Received:2019-09-22 Published:2020-11-30

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Abstract: The chemical constituents of ethyl ecetate fraction of Blumea riparia (Bl.) DC. were isolated and purified by repeated silica gel column chromatography and recrystallization methods, and 11 compounds were obtained. These structures were identified by physicochemical properties and spectral analyses as friedelin (1), friedelino (2), β-sitosterol (3), 5-hydroxy-7, 3′, 4′-trimethoxyflavone (4), quercetin (5), luteolin (6), dibutyl phthalate (7), protocatechuicaldehyde (8), porotcateehuie acid (9), caffenic acid (10), salieylic acid (11). Compounds 1,2,4 and 7 were obtained from this plant for the first time.

Key words: Blumea riparia (Bl.) DC., ethyl acetate fraction, sterols, flavonoid, organic acids, chemical constituents

CLC Number: 

  • O629
[1] 国家中医药管理局《中华本草》编委会. 中华本草(第七册)[M]. 上海:上海科学技术出版社, 1999:745-746.
[2] 广西壮族自治区革委会卫生局. 广西本草选编(上册)[M]. 南宁: 广西人民出版社, 1974:925.
[3] 黄燮才. 广西民族药简编[M]. 南宁: 广西壮族自治区卫生局药品检验所, 1980:236.
[4] 韦玥吟, 谢晓琴, 刘思彤, 等. 壮药滇桂艾纳香与中药艾纳香的化学成分及药理作用研究概况[J]. 中国民族民间医药, 2018, 27(18):55-57.
[5] 曹家庆, 孙淑伟, 陈欢, 等. 滇桂艾纳香黄酮类化学成分的研究[J]. 中国中药杂志, 2008, 33(7):782-784.
[6] 曹家庆, 王亚男, 周玉枝, 等. 滇桂艾纳香化学成分的分离与鉴定(Ⅱ)[J]. 中国药物化学杂志, 2008, 18(6):449-451.
[7] 许子竞, 林翠梧. 滇桂艾纳香多糖BRP的结构解析[J]. 化学学报, 2011, 69(9):1101-1106.
[8] 许子竞, 刘茜, 舒群威, 等. 滇桂艾纳香多糖的分离纯化及单糖组成分析[J]. 湖南师范大学自然科学学报, 2017, 40(1):65-70.
[9] 宁小清, 卢汝梅, 黄丽贞, 等. 壮药白花九里明化学成分研究[J]. 中药材, 2016, 39(11):2536-2538.
[10] 廖敏富, 林翠梧, 黄丽, 等. 滇桂艾纳香水溶性多糖BRP-B的分离纯化及止血活性[J]. 应用化学, 2011, 28(1):83-86.
[11] 许子竞, 林翠梧, 廖敏富. 新的滇桂艾纳香寡糖BROS结构分析[J]. 有机化学, 2011, 31(11):1811-1819.
[12] HUANG L, LEI T, LIN C W, el at. Blumeaxanthene II, a novel xanthene from Blumea riparia DC[J]. Fitoterapia, 2010, 81(5):389-392.
[13] 马芝玉, 林翠梧, 黄克建, 等. 滇桂艾纳香茎和叶中挥发性化学成分的HS-SPME-GC-MS分析[J]. 中山大学学报(自然科学版), 2009, 48(1):46-50.
[14] 董伟. 滇桂艾纳香超临界萃取物成分分析及在卷烟中的应用[J]. 食品工业, 2009(2):55-56.
[15] 姜建萍. 壮药滇桂艾纳香止血效应的实验研究[D]. 长沙:湖南中医药大学,2010.
[16] 姜建萍,陈美安,马雯芳,等. 滇桂艾纳香对动物离体及在体子宫平滑肌作用的影响[J].时珍国医国药,2013,24(2):312-313.
[17] 吴凌莉,刘扬,陈美红, 等. 鹅不食草的化学成分研究[J]. 中南药学, 2016, 14(4):351-354.
[18] 陈君, 韦建华, 蔡少芳, 等. 白花鬼针草化学成分研究[J]. 中药材, 2013, 36(3):410-413.
[19] 韦建华,西庆男,李兵, 等. 壮药青藤仔化学成分研究[J]. 广西师范大学学报(自然科学版), 2018, 36(2): 94-97.
[20] 罗国勇, 郎天琼, 周敏, 等. 粘叶莸的化学成分研究[J]. 天然产物研究与开发, 2016, 28:1520-1525.
[21] 杨秀芳, 程小伟, 马养民, 等. 老鹳草化学成分研究(Ⅱ)[J]. 陕西科技大学学报, 2015, 33(1):95-98.
[22] 侯勇, 厉博文, 张广杰, 等. 杨树花化学成分的分离鉴定Ⅱ[J]. 中国实验方剂学杂志, 2018, 24(23):77-81.
[23] 徐飞, 王晓中, 孙杨, 等. 宁夏枸杞醋酸乙酯部位化学成分研究[J]. 中草药, 2012, 43(12):2361-2364.
[24] 王召平, 朱姮, 李岗, 等. 忍冬根的化学成分与抗炎活性研究[J]. 中草药, 2016, 47(14):2412-2417.
[25] 范亚楚, 郭中龙, 信兰婷, 等. 排钱草化学成分的研究[J]. 中成药, 2017, 39(6):1195-1198.
[26] 薛培凤, 波拉提·马卡比力, 杨雷, 等. 蒙药蓝刺头的化学成分研究[J]. 中草药, 2017, 48(19):3921-3926.
[27] 王超, 梁辉, 郭俊明, 等. 滇南狸尾豆叶的化学成分研究[J]. 中国中药杂志, 2011, 36(19):2676-2679.
[28] 姜建萍, 陈晨, 蓝仁青, 等. 滇桂艾纳香不同提取物凝血作用的比较研究[J]. 中国实验方剂学杂志, 2010, 16(1):104-106.
[29] 金晶, 向英, 吴双, 等. 妇血康颗粒对功能失调性子宫出血模型大鼠凝血功能及性激素水平的影响[J]. 中国妇幼保健, 2017, 32(13) :3040-3042.
[30] HUANG L, LIN C W, LI A Y, el at. Pro-coagulant activity of phenolic acids isolated from Blumea riparia[J]. Nat Prod Commun, 2010, 5(8):1263-1266.
[31] 赵小杰, 黄薏霏, 林莹波, 等. 植物中几种酚酸的止血与活血作用研究[J]. 亚太传统医药, 2016, 12(11):66-69.
[32] 张翠英,郭丽丽,王阶.原儿茶醛的药理研究进展[J]. 中国实验方剂学杂志, 2013, 19(23):338-342.
[33] 蓝日春, 韦宏官, 谢植轰. HPLC测定妇血康糖浆中原儿茶酸的含量[J]. 中国民族医药杂志,2012(3):47-48.
[34] 蒋冰清, 罗盛东. HPLC法测定滇桂艾纳香中原儿茶酸和原儿茶醛的含量[J]. 黑龙江农业科学, 2015(3):120-122.
[35] 王美琪, 姜建萍, 马雯芳, 等. 多成分综合评分法优化滇桂艾纳香提取工艺[J]. 中国医院药学杂志, 2018, 38(16):1690-1693.
[36] 姜建萍, 王美琪, 马雯芳, 等. 基于多种分析模式构建壮药滇桂艾纳香HPLC指纹图谱[J]. 中药材, 2018, 41(1):124-128.
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