Journal of Guangxi Normal University(Natural Science Edition) ›› 2017, Vol. 35 ›› Issue (2): 73-79.doi: 10.16088/j.issn.1001-6600.2017.02.011

Previous Articles     Next Articles

HPLC Fingerprint of Stem of Tetrastigma planicaule(Hook. f.) Gagnep.

QIU Qin,CHEN Mingwei*, ZHEN Hanshen, JIANG Lanlan,FAN Xiuchun   

  1. Guangxi University of Chinese Medicine, Nanning Guangxi 530001, China
  • Online:2017-07-25 Published:2018-07-25

PDF (PC)

223

Abstract: To study on the HPLC fingerprint of stem of Tetrastigma planicaule(Hook. f.)Gagnep. high performance of liquid chromatography(HPLC)was adopted, the separation was performed on Ultimate C18(5 μm,4.6×250 mm) column, the mobile phase was acetonitrile-0.1% acetic acid solution with a gradient elution, the detection wavelength was 258 nm, the column temperature was set at 30 ℃ and the flow rate was 1 mL/min. The data was performed with similarity evaluation system for chromatographic fingerprint of TCM(Version 2004A). In the fingerprint,12 common peaks were confirmed and the similarity of 10 batches of stem of Tetrastigma planicaule(Hook. f.) Gagnep. were above 0.9. The experiment result could provide scientific foundation for building the quality control method of Tetrastigma planicaule(Hook. f.) Gagnep.

Key words: Tetrastigma planicaule(Hook. f.) Gagnep., stem, fingerprint, HPLC

CLC Number: 

  • R284.1
[1] 广西壮族自治区食品监督管理局.壮药质量标准(第二卷)[M].南宁:广西科学技术出版社,2011:226.
[2] 周亮,黄建平,黄自云.热带雨林老茎开花:扁担藤[J].园林,2012,1:70-71.
[3] 台海川,徐荔,王娟,等.傣药扁担藤质量标准研究[J].中国民族医药杂志,2012,11:45-46.
[4] 覃迅云,罗金裕,高志刚.中国瑶药学[M].北京:民族出版社,2002:141.
[5] 江苏新医学院.中药大辞典[M]. 上海:上海人民出版社, 1986:1741.
[6] 甄汉深,梁晓乐,丘琴,等. 壮药扁担藤的性状及显微鉴别[J].中药材,2013,36(6):900.
[7] 潘乔丹,熊圆圆,陈文东, 等. 扁担藤总黄酮和总三萜提取工艺及抗氧化研究[J].中药材,2012,35(10):1679-1683.
[8] 潘乔丹,熊圆圆,陈文东, 等. 扁担藤不同极性成分抗氧化活性研究[J].中国实验方剂学杂志,2013,19(1):232-235.
[9] 李兵,廖广凤,黄业玲,等. 瑶药扁担藤乙酸乙酯部位化学成分研究[J].中药材,2014,37(4):610-611.
[10] 卢澄生,李兵.瑶药扁担藤的化学成分预试验研究[J].广西中医学院学报,2011,14:43-44.
[11] 邵加春,何翠红,雷婷,等.瑶药扁担藤化学成分的研究[J]. 中国药学杂志, 2010, 21(45):1615-1617.
[12] 曾立,罗辉,李庚喜,等.瑶药化学成分及其资源开发[J].中国野生植物资源,2011,30(5):23-25.
[13] 刘焕蓉,郭志强,秦雪梅.山西道地药材黄芪石油醚提取物指纹图谱研究[J].广西师范大学学报(自然科学版),2003,21(3):200-201.
[14] 丘琴,甄汉深,陈明伟,等.壮药龙利叶茎HPLC 指纹图谱研究[J]. 广西师范大学学报(自然科学版),2016,34(2):116-121.
[15] 胡坤,赵书林,李舒婷,等.罗汉果的毛细管电泳指纹图谱研究[J]. 广西师范大学学报(自然科学版),2008,26(2):84-87.
[1] ZHENG Tao, ZHOU Xinran, ZHANG Long. Global Asymptotic Stability of Predator-Competition-Cooperative Hybrid Population Models of Three Species [J]. Journal of Guangxi Normal University(Natural Science Edition), 2020, 38(5): 64-70.
[2] LÜ Xiaojun, ZHAO Kaihong, LI Rui. Multiple Positive Periodic Solutions of a Discrete Non-autonomousPlankton Allelopathy System [J]. Journal of Guangxi Normal University(Natural Science Edition), 2020, 38(4): 66-73.
[3] GE Yifei, ZHENG Yanbin. Private Information Retrieval Schemes with Erasure-correcting or Error-correcting Properties [J]. Journal of Guangxi Normal University(Natural Science Edition), 2020, 38(3): 33-44.
[4] ZHANG Erli, XING Yuqing. Bifurcation of Limit Cycle for Non-Hamilton System with Invariant Straight Lines [J]. Journal of Guangxi Normal University(Natural Science Edition), 2020, 38(3): 45-51.
[5] GUAN Shuiqing, ZHOU Gailian, DONG Jingjing, LIN Qinghua, HUANG Pan, WANG Qian. Simultaneous Determination of Five Nucleosides in Pheretima aspergillum (E. Perrier) by HPLC [J]. Journal of Guangxi Normal University(Natural Science Edition), 2020, 38(3): 85-91.
[6] CHEN Xiong, ZHU Yu, FENG Ke, YU Tongwei. Identity Authentication of Power System Safetyand Stability Control Terminals Based on Blockchain [J]. Journal of Guangxi Normal University(Natural Science Edition), 2020, 38(2): 8-18.
[7] LIU Xin, LUO Xiaoshu, ZHAO Shulin. Active Disturbance Rejection Control of Three-AxisStabilized Platform Based on BP Neural Network [J]. Journal of Guangxi Normal University(Natural Science Edition), 2020, 38(2): 115-120.
[8] GAO Hongjuan, HAN Huiqing, LUO Xuqiang, LI Jinyan, CHEN Mengling, ZHANG Xinding. Effects of Land Use Change on Freshwater Ecosystem Services in Guizhou, China [J]. Journal of Guangxi Normal University(Natural Science Edition), 2020, 38(1): 157-163.
[9] LI Jiankang,WEI Duqu,LUO Xiaoshu,QIN Yinghua. Study on Chaotic Synchronization Control of Distributed Generation System and Inductive Load Network [J]. Journal of Guangxi Normal University(Natural Science Edition), 2019, 37(3): 33-41.
[10] HE Dongping,HUANG Wentao ,WANG Qinlong. Limit Cycle Flutter and Chaostic Motion of Two-Dimensional Airfoil System [J]. Journal of Guangxi Normal University(Natural Science Edition), 2019, 37(3): 87-95.
[11] HONG Lingling, YANG Qigui. Research on Complex Dynamics of a New 4D Hyperchaotic System [J]. Journal of Guangxi Normal University(Natural Science Edition), 2019, 37(3): 96-105.
[12] ZHANG Yijin. Random Dynamics for Stochastic Delay Lattice Systems in Xρ Space [J]. Journal of Guangxi Normal University(Natural Science Edition), 2019, 37(3): 106-110.
[13] CHEN Xu, LIANG Chengqin. Spectral Features, α-glucosidase Inhibitory Activities, Antioxidant Activities and Quantitative Determination of Mogroside ⅡA of Siraitia grosvenorii [J]. Journal of Guangxi Normal University(Natural Science Edition), 2019, 37(3): 132-141.
[14] HUANG Honghong , QIU Qin,ZHEN Dandan,ZHEN Hanshen,FAN Xiuchun, YU Lifeng. HPLC Fingerprint of Leaf of Sauropus rostratus Miq. from Different Places [J]. Journal of Guangxi Normal University(Natural Science Edition), 2019, 37(3): 142-147.
[15] MIAO Xinyan, ZHANG Long, LUO Yantao, PAN Lijun. Study on a Class of Alternative Competition-Cooperation Hybrid Population Model [J]. Journal of Guangxi Normal University(Natural Science Edition), 2018, 36(3): 25-31.
Viewed
Full text


Abstract

Cited
  Shared   
  Discussed   
No Suggested Reading articles found!
Copyright © Journal of Guangxi Normal University(Natural Science Edition), All Rights Reserved.
Tel: 0773-5857325　E-mail: gxsdzkb@mailbox.gxnu.edu.cn
Powered by Beijing Magtech Co. Ltd