ICP-MS法测定中药鸡血藤中28种元素

Journal of Guangxi Normal University(Natural Science Edition) ›› 2013, Vol. 31 ›› Issue (1): 76-81.

Previous Articles Next Articles

Determination of 28 Elements of Spatholobus suberectus Dunn by ICP-MS

SU Jun¹, DUAN Yu-lin¹, LÜ Shi-jun¹, LIU Dong-cheng²

1.Guangxi Product Quality Supervision and Inspection ResearchInstitute,Nanning Guangxi 530007,China;
2.Chemistry and Chemical Engineering,Guangxi Normal University,Guilin Guangxi 541004,China

Received:2012-09-16 Online:2013-03-20 Published:2018-11-26

Abstract

Abstract: In order to study the relationship between trace elements of Spatholobus suberectus dunn and efficacy,and continue to develop andutilize Spatholobus suberectus dunn,ICP-MS was applied to simultaneously determine 28 elements concealed spatholobus suberectus dunn for the first time.The sample was dissolved with microwave digesting,wet digesting and dry ashing.Thematrix effect was corrected by the in-line addition of internal standard (Be,Y,Sc,In,Re).The analysis method is simple,rapid,accurate and fiting to the determination of elements in Chinese herbs.The detection limits of these element werein the range of 0.01～0.8 μg/L.The relative standards (RSD) were in the range of 0.11%～2.57%,and the recoveries were in the range of 94.00%～110.00%.The results show that large amounts of elements are embodied in spatholobus suberectus dunn.There are 13 kinds of element content in 2 mg/kg above.The contents of Ca、Kand Mg are in conformation with the medical effects of spatholobus suberectus dunn.It can provide scientific basis for further development of the effect of Spatholobus suberectus dunn.

Key words: ICP-MS, elements, Spatholobus suberectus dunn

CLC Number:

O657.63

SU Jun, DUAN Yu-lin, LÜ Shi-jun, LIU Dong-cheng. Determination of 28 Elements of Spatholobus suberectus Dunn by ICP-MS[J].Journal of Guangxi Normal University(Natural Science Edition), 2013, 31(1): 76-81.

References

[1] 孟君,郭全海,蒋玲,等.HG-ICP-AES法测定山豆根中的微量元素[J].广西师范大学学报:自然科学版,2009,27(2):69-73.
[2] 满微,张秀慧,王寅鹏,等.中药中微量元素的测定研究进展[J].世界元素医学,2011,1:18-21.
[3] 曹治权.微量元素与中医药[M].北京:中国中医药出版社,1993:132.
[4] 李云,李丹,黄凯,等.蕨根总黄酮提取工艺研究及其微量元素测定[J].广西师范大学学报:自然科学版,2009,27(2):64-68.
[5] 张少梅,王恒山,陈振锋,等.ICP-MS测定广西巴豆不同部位中的十种微量元素[J].广西植物,2009,29(6):774-776.
[6] 国家药典委员会.中华人民共和国药典[M].北京:化学工业出版社,2005:134.
[7] 中国科学院中国植物志编辑委员会.中国植物志:第四十一卷[M].北京:科学出版社,1995:192-193.
[8] 王强,徐国均.道地药材图典:中南卷[M].1版.福州:福建科学出版社,2003:102-103.
[9] 国家中医药管理局中华本草编辑委员会.中华本草[M].上海:上海科学技术出版社,2005:656-658.
[10] 陈东辉,罗霞,余梦瑶,等.鸡血藤煎剂对小鼠骨髓细胞增殖的影响[J].中国中药杂志,2004,29(4):68-71.
[11] 戴关海,杨锋,沈翔,等.鸡血藤对S₁₈₀小鼠细胞毒细胞活性影响的实验研究[J].中国中医药科技,2001,8(3):33-34.
[12] KANG In-cheol,KIM Seung-ae,GYU Yong-song.Effects of the ethylacetate fraction of Spatholobi caulis on tumour cell aggregation and migration[J].Phytotherapy Research,2003,17(2):163-167.
[13] GUO Jin-peng,PANG Ji,WANG Xin-wei,et al.In vitro screening oftraditionally used medicinal plants in China against enteroviruses[J].World J Gastroenterol,2006,12(25):4078- 4081.
[14] 邱丽,施意华,杨仲平,等.ICP-MS法测定隐伏矿植物中的多种微量元素[J].广西科学院学报,2010,26(3):303-305.
[15] 中华人民共和国卫生部,中国国家标准化管理委员会.GB/T5750.6—2006生活饮用水标准检验方法金属指标[S].北京:中国标准出版社,2006.
[16] 中国质量监督检验总局.JJF 1159—2006四极杆电感耦合等离子体质谱仪校准规范[S].北京:中国标准出版社,2006.

Metrics

Viewed

Full text

Abstract

Cited

Shared

Discussed

Comments

Recommended 0

No Suggested Reading articles found!

Determination of 28 Elements of Spatholobus suberectus Dunn by ICP-MS

Abstract

Cite this article

share this article

References

Related Articles 2

Metrics

Comments

Recommended 0

[1]	PU Ling, LI Hai-chao, PU Yu, JIANG Hong-xia. Principal Component Analysis of Trace Elements in 12 Commonly Used Chinese Herbal Medicines [J]. Journal of Guangxi Normal University(Natural Science Edition), 2014, 32(4): 96-100.
[2]	YANG Guang-hui, XIANG Shu-wen. Generic Stability on Generalized Maximal Elements [J]. Journal of Guangxi Normal University(Natural Science Edition), 2013, 31(1): 54-56.